155: 423 Design of Separation Processes Fall 2001


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Lectures: Wed 11:30am-12: 50pm, Frid 1:10pm-2: 30pm SEC 210

Instructor: Marianthi G. Ierapetritou

Engineering C-137

Busch Campus

tel: (732) 445-2971, email: marianth@sol.rutgers.edu

Teaching Assistant: Eric Semler Office hours: to be announced

Email: ej_semler@yahoo.com

Tel: 445-5511

Office Rm#: C001

Course Description: The purpose of this course is to provide fundamental instruction on the mathematics and science associated with separation processes. This course will review techniques required to design the classical separation processes such as distillation, absorption and extraction. Rigorous and short-cut methods will be covered.

Course Objectives:

  1. Educate students to structure and solve the problems arising in all chemical engineering industry related to design of separation processes.
  2. Learn basics of chemical engineering separation processes.
  3. Learn the use of computer software used for the design of separation processes.

Textbooks:

Separations in Chemical Engineering: Equilibrium-Staged Operations

By P.C, Wankat,

Published by Prentice Hall, 1988.

Separation Process Principles

By J.D. Seader and E.J. Henley.

Published by John Wiley & Sons, 1998.

Software:

CHEMCAD: This is a steady-state process simulator for chemical engineering design. It performs mass and energy balances, equipment sizing and costing and draws flow diagrams. It has an extensive thermodynamic property database. It is installed on all PC in the Microcomputer Lab (room C233). Login and run it by using the command CHEMCAD.

Admission Tickets:

To improve class participation, there will be an "admission ticket" due at the start of the class on Wednesdays for both those enrolled and for those auditing. The ticket is the solution (or attempt at a solution) of a short problem. It will be not be graded but failure to hand it in will be considered in the assessment of "class participation". For our guest auditors, failure to hand in the ticket will be considered bad form and punishable by not more than a slap on the wrist. These problems will be available on the web site at least two days ahead of the class. In many cases the problem will be worked during the lecture. For Friday classes the homework will be also serve as admission tickets.

Assessment: Homework and Admission Tickets: 30%, Exams: 40%, Design Project: 30%

Topics covered:

Week

Date

Topic

Chapter

1

Sept. 5

Course Organization-Introduction to Separation Processes

1

 

Sept. 7

Review of Vapor-Liquid Equilibria

Bubble-point and Dew-point Calculations

2

 

 

 

 

2

Sept. 12

Flash Distillation

3

 

Sept. 14

Flash Distillation

 

 

 

 

 

3

Sept. 19

Multi-stage Distillation

4

 

Sept. 21

Introduction to CHEMCAD (Dr. A. Constantinides)

 

 

 

 

 

4

Sept. 26

Binary Systems – McCabe-Thiele method

6

 

Sept. 28

Binary Systems – McCabe-Thiele method

 

 

 

 

 

5

Oct. 3

Binary Systems – Enthalpy Concentration Diagram Method

6

 

Oct. 5

Binary Systems – Enthalpy Concentration Diagram Method

 

 

 

 

 

6

Oct. 10

First Exam

 

 

Oct. 12

Multi-component Systems Exact methods

Design Project assignment

8

 

 

 

 

7

Oct. 17

Multi-component Systems Exact methods

8

 

Oct. 19

Multi-component Systems Shortcut methods

9

 

 

 

 

8

Oct. 25

Multi-component Systems Shortcut methods

9

 

Oct. 26

Complex Distillation Methods

10

 

 

 

 

9

Oct. 31

Complex Distillation Methods

10

 

Nov. 2

Staged/Packed Column Design(Dr. Mark Andrekovich from BOC)

12/13

 

 

 

 

10

Nov. 7

Staged/Packed Column Design

12/13

 

Nov. 9

Second Exam

 

 

 

 

 

11

Nov. 14

Absorption and Stripping

15

 

Nov. 16

Absorption and Stripping

 

 

 

 

 

12

Nov. 21

Liquid-Liquid Extraction

 16

 

Nov. 23

Happy Thanksgiving!!!!

 

  

 

 

 

13

Nov. 28

Liquid-Liquid Extraction

16

  

Nov. 30

Membrane Separations

14(Seader/Henley)

  

 

 

  

14

Dec. 5

Membrane Separations

14 (Seader/Henley)

  

Dec. 7

Adsorption

15 (Seader/Henley)

  

 

 

 

15

Dec. 12

Adsorption

15 (Seader/Henley)

  

Dec. 14

Design Project Due

 



marianthi@sol.rutgers.edu
04/23/02